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SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE, Official Publication of Sant Gadge Baba Amravati University, , PART – TWO, ____________________________________________________________________________________________________________________________________________________________________________________, , Thursday, the 27th April, 2017, NOTIFICATION, No. : 28/ 2017, , Date : 27/04/2017, , Subject : I) Continuation of Prospectus No.2016123 prescribed for B.Sc.Final for the, Session 2017-18., II) Introduction of new subjects i.e. Forensic Science & Animation for B.Sc. Final, from the session 2017-18., I) It is notified for general information of all concerned that the Prospectus of B.Sc.Final (Sem-V & VI), bearing No.2016123 prescribed for the Academic Session 2016-17 shall continue for the session 2017-18, along with the following substitutions/additions., “The syllabi of B.Sc.Final Sem-V ‘5S Mathematics, Paper IX & Paper X’ printed on page Nos.1 to 2 and, B.Sc. Final Sem-VI ‘6S Mathematics, Paper XI & Paper XII’ printed page Nos. 2 to 8 be substituted by the, Appendix-A appended with this Notification.”, II) It is further notified for general information of all concerned that the authorities of the University have, introduced the new subject i) Forensic Science & ii) Animation, at B.Sc. Final (Sem-V & VI) from the, session 2017-18 as –, i) ‘‘5S Forensic Science (Forensic Psychology)’’ and “6S Forensic Science (Digital & Cyber Forensics)”, as given in Appendix-B,, ii) ‘‘5S Animation (Advanced Graphics and Special Effects)’’ and “6S Animation (Introduction to 3D, Animation)” as given in Appendix-C appended with the notification., Sd/(Dr.A.P.Deshmukh), Registrar, Sant Gadge Baba Amravati University, , Appendix – A, Syllabus Prescribed for B.Sc. Final (Semester-V & VI) Examination to be implemented, from the Academic Session 2017-18, , Semester V, 5S Mathematics Paper –IX, (Mathematical Analysis), Unit–I, , :, , Unit II :, Unit-III :, Unit-IV :, Unit-V, , :, , Riemann Integral: Integrability of continuous and monotonic functions, the fundamental theorem, of integral calculus, mean value theorem of integral calculus., Improper integrals and their convergence, comparison and limit tests.Beta and gamma functions., Continuity and differentiability of complex function, analytic function, Cauchy-Riemann, equations, harmonic and conjugate functions, Milne-Thomson method., Elementary function, mapping by elementary function, Mobius transformation, fixed point, cross, ratio, inverse and critical points, conformal mapping., Metric spaces: Definition and examples of metric spaces, neighbourhood, limit point, interior, point, open and closed sets, Cauchy sequences, completeness., , Reference Books :, 1. R. R. Goldberg:Methods of Real Analysis, Oxford IBH publishing Co. New Delhi, 1970., 2. T. M. Karade, J. N. Salunke, K. S. Adhav, M. S. Bendre : Lectures on Analysis, Sonu Nilu Publication,, Nagpur., 3. Walter Rudin: Principles of Mathematical Analysis, International students edition (Third edition ), 4. T. M. Apostol :Mathematical Analysis, Narosa Publishing House, New Delhi, 1985.,, 5. S. Lang : Undergraduate Analysis, Springer-Verlag New York, 1983., 6. D. Somasundaram & B. Choudhari : A First Course in Mathematical Analysis, New Delhi. 1997., 7. Shanti Narayan : A Course of Mathematical Analysis, S. Chand & Co., New Delhi., 8. P. K. Jain & S. K. Kaushik : An Introduction to Real Analysis, S. Chand & Co. New Delhi, 2000., 9. R. V. Churchiln and J.W.Brown, Complex Variables and Applications, 5th Edition, McGraw Hill, New, York,1990, 10. Mark J Ablowitz and : A.S. Fokas, Complex Variable Introduction and Application, Cambridge University, Press , South Asian Edition ,1998., 11. Shanti Narayan : Theory of functions of Complex Variable,,S.Chand and Co. New Delhi., 12. E.T.Coption,:Metric Spaces, Cambridge University Press ,1968., 13. P.K.Jain and K.Ahmed ,:Metric Spaces ,Narosa Publishing House, New Delhi 1996., 14. G.F.Simmons :Introduction to Topology and Modern Analysis, McGraw Hill, New York,1963., 15. T. M. Karade, J. N. Salunke, A. G. Deshmukh, M. S. Bendre: Lectures on Advanced Calculus, Sonu-Nilu, Publication, Nagpur., 16. Murray R. Spiegel :Theory and Problems of Advanced Calculus, Schaum Outline Series., 17. S. C. Malik and Arora : Mathematical Analysis, Wiley Estern Ltd., New Delhi., ----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 42, -----------------------------------------------------------------------------------------------------------------------------------------

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 43, ----------------------------------------------------------------------------------------------------------------------------------------Semester V, 5S Mathematics Paper –X, ( Mathematical Methods ), Unit-I, , :, , Unit-II, , :, , Unit-III :, Unit-IV :, , Unit-V, , :, , Legendre’s equation, Legendre’s polynomials, generating function of, , recurrence formulae, for, , orthogonality of Legendre’s polynomial, Rodrigue’s formula., Bessel’s equation, solution of Bessel’s equation, generating function for, , Recurrence, formulae for, . Strun-Liouville boundary value problem., Fourier series, Fourier series for odd and even functions, half-range Fourier sine series and halfrange Fourier cosine series., Laplace transform: Laplace transform of some elementary functions, existence of Laplace, transform. properties of Laplace transform. Laplace transform of derivatives and integrals,, multiplications of, and division by t, inverse Laplace transform, convolution property,, application of Laplace transform in solving ordinary and partial differential equations., Fourier Transform: Finite Fourier sine transform, inverse finite Fourier sine transform and cosine, transform, Infinite Fourier transform, infinite Fourier sine transform and cosine transform,, properties of Fourier transform, application to partial differential equations., , Reference Books :, 1), 2), 3), 4), 5), 6), 7), 8), , Erwin Kreyszig : Advanced Engineering Mathematics, John Wiley and Sons, Inc. New York, 1999., A. R. Forsyth : A Treatise on Differential Equations, Macmillan and Co. Ltd. , London., Frank Ayres : Theory and Problems of Differential Equations. McGraw Hill Book Company, 1972., B. Courant and D. Hilbert : Methods of Mathematical Physics, Vol. I & II, Wiley-interscience, 1953., T. M. Karade : Lectures on Differential Equations, Sonu-Nilu Publication, Nagpur., I. N. Sneddon : Fourier Transforms, McGrow Hill Book Co., Goel and Gupta : Integral Transforms, Pragati Prakashan , Meerut., Raisinghaniya,M.D., Integral Transform, S.Chand & Co., N.D., Semester VI, 6S Mathematics Paper -XI, (Linear Algebra ), , Unit I, , :, , Unit II, , :, , Unit III :, Unit IV, , :, , Unit V, , :, , Vector Space : Definition and example of vector spaces, subspaces, sum and direct sum of, subspaces, linear span, linear dependence, independence and their basic properties, basis , finite, dimensional vector spaces ,existence theorem for bases, invariance of the number of elements of a, basis set, dimension., Linear transformations:Linear transformation and their representation as matrices, algebra of, linear transformations, rank nullity theorem, change of basis., Dual Spaces: Dual space, bidual space and natural isomorphism, adjoint of a linear, transformation, Eigen values and eigenvectors of a linear transformation., Inner Product Spaces: Inner product spaces, Cauchy-Schwarz inequality, orthogonal vectors,, orthogonal complements, orthonormal sets and bases, Bessel’s inequality for finite dimensional, spaces,Gram Schmidt orthogonalisation process., Modules: Modules, submodules, quotient modules, homomorphism and isomorphism theorems., , Reference Books:, 1., 2., 3., 4., 5., 6., 7., 8., 9., 10., 11., 12., 13., 14., 15., 16., , I. N. Herstein: Topics in Algebra, Wiley Eastern Ltd., New Delhi,1975., N. Jocobson: Basic Algebra ,Vol. I and II W.H.Freeman,1980 (Hindustan Publishing Co.), Shanti Narayan :A Text Book Of Modern Abstract Algebra, S. Chand and Co. ,New Delhi, K. B. Datta: Matrix and Linear Algebra, Prentice Hall of India Pvt. Ltd. New Delhi,2000, P.B. Bhattacharya, S. K. Jain and S. R. Nagpal :Basic Abstract Algebra (IInd Edition) Cambridge, University Press Indian Edition,1997, K. Hoffman and R. Kunze: Linear Algebra ,IInd Edition Prentice Hall,Englewood Cliffs, New, Jersey,1971., S. K. Jain, A Gunawardhana and P. B. Bhattacharya: Basic Linear algebra with MATLAB, Key College, Publishing (Springer-Verlag), 2001., S. Kumaresan : Linear Algebra, A Geometric Approach P Prentice Hall of India Pvt. Ltd. New, Delhi,2000 ., Vivek Sahai and Vikas Bisht :Algebra, Narosa Publishing House ,1997., D. S. Malik,J. N. Mordeson and M. K. Sen :Fundamentals of Abstract Algebra ,McGraw Hill, International Edition 1997 ., T. M. Karade, J.N. Salunke, K. S. Adhav, M. S. Bendre : Lectures on Abstract Algebra. Sonu Nilu, Publication. Nagpur (IInd Publication)., John B. Fraleign : A First course in Abstract Algebra., Joseph A. Gallian: Contemporary Abstract Algebra, Narosa publishing house., P.B. Bhattacharya, S.K. Jain and S.R. Nagpaul: First Course in Linear Algebra., V. Krishnamurty , V. P. Mainru, J.L. Arrora: An Introduction to linear Algebra., L Smith: Linear Algebra, Springer-Verlag New York.

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 44, ----------------------------------------------------------------------------------------------------------------------------------------Semester VI, 6S - Paper-XII (Optional), (Graph Theory ), Unit I, , :, , Unit II, , :, , Unit III :, , Unit IV, , :, , Unit V, , :, , Graph. Application of graphs, finite and infinite graphs, incidence and degree, isolated vertex,, pendent vertex and null graph, isomorphism, subgraphs, walks, path and circuits, connected, graphs and components, Euler graph, operation on graphs, Hamiltonian paths and circuits,, travelling salesman problem., Trees, some properties of trees, pendent vertices in a tree, distance and centres in a tree, Rooted, and binary trees, On counting trees, spanning trees., Fundamental circuits, Cutsets, Some properties of cutesets, all cuteset in a graph, fundamental, circuits and cutsets, connectivity and separability, planer graphs, Kurutowski’s two graphs,, different representation of planer graph, detection of planarity., Vector space associated with a graph, circuit and cuteset subspaces, Orthogonal vectors and, spaces, Intersection and join of W and Ws ., Incidence matrix, Submatrix of A(G), Circuit matrix, Fundamental circuit matrix B, Rank of B,, an application to a switching network, cuteset matrix, path matrix, adjacency matrix, the, relationship among A f , A f and C f ., , Reference Books:, 1. Narsingh Deo: Graph Theory with Application to Engineering and Computer Science, Prentice Hall Of, India, New Delhi.,, 2. Richard Johnson- Baugh : Discrete Mathematics,Macmillan Publishing Company 886, Third Avenue, NewYork 10022, 3. Olympia Nicodemi : Discrete Mathematics,C.B.SPubl.and Distributors 485,Jain Bhavan Bholanath, NagarShahadara New Delhi-32 India, 4. Frank Harare : Graph Theory ,Narosa Publishing House ,307 ,Shiv Centre D.B.C. Sector Ku Bazar, NewBombay 400704,, 5. S.A.Choudum: A first Course In Graph Theory, McMillan India Ltd. Mercatile HouseMagazine Street, Bombay 10, 6. E.L.LIU : Elements of Discrete Mathematics, McGraw Hill Book Company,New York, 7. Seymour Lipschiutz and Marc Lipson : Discrete Mathematics ,TMH New Delhi (Schaum Outline series), IIndEdition., 8. J.N.Salunke :Boolean Algebra and Graph Theory Laxmi Publication Akot., Semester- VI, 6S Mathematics Paper- XII, (Special Theory of Relativity) ( Optional), Review of Newtonian Mechanics. Inertial frames, speed of light and Galilean relativity, relative, character of space and time, postulates of special theory of relativity, Lorentz transformation and, its geometrical interpretation, group properties of transformation., Unit –II : Relativistic Kinematics. Composition of parallel velocities, length contraction, time dilation,, transformation equation for components of velocities and acceleration of a particle, Lorentz, contraction factor. The thermodynamics of moving systems : The two laws of thermodynamics, for a moving system, the Lorentz transformation for thermodynamics quantities a) volume and, pressure b) energy c) work d) heat e) entropy f) temperature, Unit- III : Geometrical representation of space- time. Four dimensional Minkowskian space-time of, relativity , time like and space like intervals , proper time , world line, four vectors and tensors in, Minkowskian space-time ,past, present and future null cone ,basic tensors, covariant, contrvariant,, mixed , operations on tensors, outer product, inner product, quotient law., Unit- IV : Relativistic Mechanics. Variation of mass velocity, equivalence of mass and energy,, transformation equation for mass, momentum and energy, relativistic force and transformation, equations for its components, relativistic Lagrangian and Hamiltonian, the energy momentum, tensor., Unit-V : Electromagnetism: Maxwell’s equations of electromagnetic theory in vacuum, propagation of, electric and magnetic field strengths , scalar and vector potential, transformation of, electromagnetic four potential vector, transformation of charged density and current density,, Lagrangian for a charged particle in electromagnetic field, the force on a moving chargedLorentz force, Gauge transformation, four dimensional formulation of the theory, Maxwell’s, equation in tensor form, transformation for electric and magnetic field strength, energy, momentum tensor of the electromagnetic field. component of Tij in term of electric and magnetic, strength., Reference Books:, 1. C. Molar : The Theory of Relativity, Oxford Clarendon Press, 1952., 2. P. G. Bergman : Introduction to The Theory of Relativity, Prentice Hall of India,Pvt.Ltd.1969., 3. T.M.Karade, K.S.Adhav and M.S.Bendre: Lectures on Spacial Theory of Relativity ,Sonu Nilu, Publication, Nagpur, 4. J. L. Anderson :Principles of Relativity Physics, Academic Press, 1967., 5. V. A. Ugarov : Special Theory of Relativity, Mir Publishers, 1979., 6. R. Resnick :Introduction to Special Relativity Wiley Eastern,Pvt.Ltd.1972., Unit -I, , :

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 45, ----------------------------------------------------------------------------------------------------------------------------------------Semester VI, 6S Mathematics Paper- XII, (Mathematical Modelling) ( Optional), Unit-I, , :, , Unit-II, , :, , Unit-III :, Unit-IV :, Unit-V, , :, , The Process of applied mathematics. Setting of First-order differential equations – Qualitative, Solutions Sketching., Difference and Differential Equation growth models – single species population models., Population growth- An age structure model. The spread of Technological innovation., Higher order linear models - A model for the detection of diabetes. Combat modes. Traffic, models - Car-following models. Equilibrium speed distributions., Non-linear population growth models. Prey-Predator models. Epidemic growth models. Models, from political Science -Proportional representation - cumulative voting, comparison voting., Applications in Ecological and Environmental subject areas -Urban waste water management, planning., , References Books :, 1) Vol.1. Differential equation models, Eds. Martin Braun, C.S.Coleman, D.A.Drew., 2) Vol.2. Political and Related Models. Steven J. Brams, W.F. Lucas, P.D.Straffin (Eds), 3) Vol.3. Discrete and System models.W.F.Lucas, F.S.Roberts, R.M.Thrall., 4) Vol.4. Life Science Models. H.M.Roberts & M.Thompson., 5) All Volumes published as modules in Applied Mathematics, Springer-Verlag,1982., *****, , Appendix-B, Syllabus of B.Sc. Part- III (Semester- V & VI) (Forensic Science), 5S Forensic Science (Forensic Psychology), (Effective from session 2017-18), The examination in Forensic Science of Fifth semester shall comprise of one theory paper, internal, assessment and practical examination. Theory paper will be of 3 Hrs. duration and carry 80 marks. The internal, assessment will carry 20 marks. The practical examination will be of 6 to 8 hours duration and carry 50 marks., The following syllabus is prescribed on the basis of six lectures per week and 6 practical periods per, batch per week. Each theory paper has been divided into 6 units. There shall be one question in every unit with, internal choice for each of 12 marks & one compulsory question covering all the syllabus of Semester-III (8, marks)., B.Sc. Part- III (Semester- V), 5S Forensic Science (Forensic Psychology), Total Lectures: 84, Marks: 80, Note: Figures to the right hand side indicate number of lectures., Unit I, , :, , The Science of Psychology, 14L, Concepts of psychology- Definition of psychology, goals of psychology, History of psychologyDevelopment of psychology, role of psychologist, Different perspectives in Psychology- Modern, perspectives, Humanistic, behaviouristic, cognitive, psychodynamic. Types of psychology, professions- Psychiatrist, Psychologist, Counsellor. The science and research methods- Interview,, observation, case study method Professional and Ethical issues in psychology- APA code of, conducts for Psychologist., Unit II : Theories of Personality, 14L, Understanding personality: Definition- mainly all port’s definition, stressing uniqueness, enduring, characteristics, temperament. Approaches – Psychodynamic (Freud, Jung & Adler), Humanistic, (Rogers & Maslow) Dispositional approaches – Type (Jung. Type A & B, Rotter and Big – 5 and, Trait (Catelli) Behavioural Approaches - Locus of control and Social learning theory. Assessment, of personality – Questionnaires, Rating Scales and Projective tests, biological model assessment, of personality. Psychological theories: Learning behavioural theory, Psycho analytic theory,, Cognitive theory, REBT., Unit-III :, 14L, A) The Content of Forensic Psychology, [4L], History of Forensic Psychology (Historical Perspective), Defining Forensic Psychology., Importance of Forensic Psychology., B) Applying Social Psychology in the interpersonal aspects of legal system, [5L], Before the trial begins: 1. Effect of police procedure and media coverage, 2. Eye Witness Testing:, Problems and Solutions. The Central participation in trial, Effect of Attorney, Judges, Jurors, and, Defenders., C) Legal Aspects of Forensic Psychology, [5L], Introduction. Historical Background Survey into Psychological evidence in court. Ethical and, Professional Issues. The role of Forensic Psychology. Civil cases, Criminal cases., Unit IV : Personality Disorders, 14L, Defining and Diagnosing Personality Disorders. Odd-Eccentric Personality Disorders. DramaticEmotional Personality Disorders. Anxious-Fearful Personality Disorders. Alternative, Conceptualization of Personality Disorder. Stress and Health: Stress Factors in the stress reaction., Coping with the stress. Statistics in Forensic Psychology. Descriptive Statistics, Inferential, Statistics.

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 46, ----------------------------------------------------------------------------------------------------------------------------------------Unit V :, , 14L, A) Essentials of Forensic Psychology, [6L], Development of forensic psychology, Ethical standards of forensic psychology, Scientific, methods used in forensic psychology, Importance of study of forensic psychology., B) Causes of criminal behaviour and Psychological theories, [8L], Psychological Factor & delinquency, ADHD & conduct disorder, Psychopathy & antisocial, personality disorder, Sexual disorder, Substance abuse, Treatment., , Unit VI, , :, , Investigative psychology, 14L, Criminal psychological profiling-Nature, definition. Psychological tests used Criminal, psychological profiling, Psychological autopsy, Forensic hypnosis (Narco analysis), Polygraph,, Stalking, The Psychology of violence., Semester- V, 5S Forensic Science (Forensic Psychology), , Total Laboratory sessions: 21, Marks: 50, List of Practical's, 1. Reaction Time: Comparison of RT under simple and disjunctive conditions., 2. Concept Formation: Comparison of the speed of development of 2 types of concepts., 3. Thinking and Problem Solving., 4. Correlation coefficient Raven’s Standard Progressive Matrices (SPM) and Abstract Reasoning (AR), scores., 5. Eysenck Personality Questionnaire,  Conduction of Psychological tests – Intelligence test:, 6. Wechsler’s adult intelligence scale, 7. Wechsler’s intelligence scale for children, 8. Standard progressive matrices by Raven.,  Personality test:, 9. Eyscenk personality inventory, 10. 16.P.F. by R.B. Cattle, 11. Thematic apperception test., 12. Rorschak inkblot test, 13. Aptitude test: Differential aptitude test., 14. Measuring Locus of control., Distribution of Marks for Practical Examination., Time: 4 – 6 hours, Marks: 50, Exercise- I, ……….., 12, Exercise- II, ……….., 12, Exercise- III, ……….., 12, Viva-Voce, .………., 07, Record, .………., 07, -----------------------Total:, 50, Books Recommended:, 1. General Psychology by Cicarelli., 2. General Psychology by Vipan Kumar., 3. Behavior Modification, Martin Garry,(2002),7th edi., 4. Introduction to Psychology, Morgan, King, Weiss and Schopler, VII edition, (1989) McGraw Hill, India., 5. Abnormal psychology & modern life,Carson RC & Butcher JN (10th Ed) Harper-Collins NY., 6. Introduction to Psychology, Atkinson and Atkinson, (1975) Oxford IBH Publishing Co. Pvt. Ltd., 7. Introduction to Forensic Science in Crime Investigation By Dr.(Mrs.) Rukmani Krishnamurthy., 8. Experimental Psychology: An Introduction. Underwood. B. J. (1968). NewYork: Appleton Century Croft, Ltd., 9. Psychological Testing. Anastasi, A.& Urbina, S. (1997) (7th ed.) International edition, Prentice Hall, International, Inc., 10. Forensic Psychology, Graham J.Towel & David A. Crighton., 11. Psychological testing and the selection of police officers: BPS BLACKWELL Cochrane, R. E., Tett, R. P.,, Vandecreek, L. (2003). A National Survey. Criminal Justice and Behavior, 30(5), 511-537., 12. Criminal psychological profiling: Validities and abilities. Kocsis, R. N. (2003), International Journal of, Offender Therapy and Comparative Criminology, 47(2), 126-144., 13. Prof. Paranjape N. V., Criminology and Penology, Central Law Publication, Allahbad., 14. Barlow & Durand. V. M. (2005) Abnormal Psychology, 6th Ed. New Jercy., Semester- VI, Forensic Science, 6S Forensic Science (Digital and Cyber Forensics), Total Lectures: 84, Note: Figures to the right hand side indicate number of lectures., , Marks: 80

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 47, ----------------------------------------------------------------------------------------------------------------------------------------Unit I, , :, 14L, A) Introduction to Operating System, [5L], Basics of Operating System, memory structure, concurrency, scheduling, synchronization &, memory management, process description and control. Introduction to Operating System (Batch, Operating System, Distributed operating system, etc) Introduction to Windows and Linux, operating System., B) Introduction to Internet, [5L], World Wide Web, E-mails, Chat, Search Engines, Network Security–Threats, Vulnerabilities,, Access Control, Malicious Code (Virus, Worms, Trojans, etc.) Introduction to Security and, Security model (CIA triad)., C) Cyber Crime & Digital Evidence, [4L], What is cyber crime, types of cyber crimes, Digital evidence, Digital Vs Physical evidence, nature, of digital evidence, precautions while dealing with digital evidence., Unit II :, 14L, A) Incident Response, [8L], Introduction to Incident Response Process (What is Computer Security Incident, What are the, goals of Incident Response, Who is involved in Incident Response Process, Incident Response, Methodology, Formulate a Response Strategy, Investigate the Incident.),Preparing For Incident, Response, Overview of Preincident Preparation, Identifying Risk, After Detection of an Incident., B) Cyber Forensic Tools and Utilities, [6L], Introduction, Examining a Breadth of Products, Cyber Forensic Tools Good, Better, Best: What’s, the Right Incident Response Tool for Your Organization?, Tool Review Forensic Toolkit,, EnCase, Cyber check suites, what is disk Imaging etc. Specifications for Forensic tools Tested, Unit III, 14L, A) Evidence Collection and Analysis Tools, [7L], Volatile and Non volatile, Evidences collection (Safeback, Gettime, FileList,Filecvt and Excel,, Getfree, Swapfiles and Getswap ,GetSlack, Temporary Files), Detailed Procedures for Obtaining, a bit stream backup of hard drive, File System (Details of File system, Data Structure Of File, System, Data Recovery in Different file system), B) Biometrics, [7L], Introduction to Biometrics, What is Biometrics, Why use Biometrics, Model of Biometric system, Various types of Biometric methods, User Acceptance, Evaluating Accuracy, Advantages &, disadvantages General Biometric System (Identification and Verification), General Architecture, Comparison of different Biometric Technologies, What makes Biometrics difficult., Unit IV, , :, , Unit V, , :, , Unit VI, , :, , Data and Evidence Recovery, 14L, Computer and cyber forensic basics, Cell Phone / Mobile Forensics, Blue-Tooth, Computer, Ethics and Application Programs. Data and Evidence Recovery-Formatted Partition Recovery,, Data Recovery Tools, Data Recovery Procedures and Ethics, Fine Transfer Protocol (FTP),, Preserve and safely handle original media, Document a "Chain of Custody", Complete time line, analysis of computer files based on file creation, file modification and file access, Recover, Internet Usage Data, Recover Swap Files/Temporary Files/Cache Files, Introduction to Encase, Forensic Edition, Forensic Tool Kit (FTK) etc, Use computer forensics software tools to cross, validate findings in computer evidence related cases., Cyber Forensics Investigation, 14L, Technical issues – Security Technologies: Certification and key, Distribution, Cryptographic, Applications, Digital Signature Protocols for Transactions, SSL-Secure, Socket Layer, SETSecure, Electronic Transaction. Cyber Forensics Investigation- Introduction to Cyber Forensic, Investigation, Investigation Tools, eDiscovery, Digital Evidence Collection, Evidence, Preservation, E-Mail Investigation, E-Mail Tracking, IP Tracking, E-Mail Recovery, Encryption, and Decryption methods, Search and Seizure of Computers, Recovering deleted evidences,, Password Cracking., Information technology law, 14L, IT Act 2000: Scope, Objectives, E- Governance, Creation, Recognition and Verification of, Digital Signature Digital Signature and Penalties under IT Act 2000, Certifying Authority and, Controller. Emerging trends in Information Technology law. Ammendment of IT act 2008., Semester- VI, 6S Forensic Science (Digital and Cyber Forensics), , Total Laboratory sessions: 21, Marks: 50, List of Practicals, 1. Working with windows file (creation, modification, deletion, attributes) folder (creation, nesting,, attributes), 2. Working with Linux- file (Creation, modification, deletion, attributes), folder (creation, nesting attributes)., 3. Working with external storage devices using windows- Reading and writing data on floppy, CD,DVD,, USB thumbdrive, 4. Working with external storage devices using Linux-reading writing data on floppy, CD, DVD, USB,, thumb drive., 5. Understanding LAN-client/server, user creation, password protection., 6. Use of internet- visiting websites with given URL, searching information using search engine.

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 48, ----------------------------------------------------------------------------------------------------------------------------------------7., 8., 9., 10., 11., 12., 13., 14., 15., 16., 17., 18., 19., 20., 21., 22., 23., 24., , Use of E-mail, creating e-mail, sending and receiving e-mails with attachments., Tracing E-mail, finding senders IP address, of received email, tracing route of email received using tool, available on internet, e.g. Visual Trace Route etc., Identification, Seizure, Search of Digital media, Evidence Collection, Demonstration of various Forensic tools like Partition magic, Encase etc., Data Recovery, Deleted File Recovery viewing small Disk., Demonstration of Concealment Techniques (Cryptography PGP), Formatting NTFS and EX2, EX3., Case study of Biometric Techniques, Data Recovery integrated with forensic technology (2 nos.), Mobile Forensic using cell phone forensic suit (2 nos.), Computer Forensic Investigation Tools, Digital Forensics investigation Tools (2 nos.), Creation & verification of Digital Signature (2 nos.), Network Analysis (2 nos.), Detail Analysis of E-mail, E-Mail Investigation, E-Mail Tracking, IP Tracking, E-Mail Recovery (2 nos.), Working on En Case Software (2 nos.), Image processing using tools like, Photoshop, Corel Photo paint etc. (2 nos.), E-Commerce (E-shopping of any product to understand the transaction and security issues) (2 nos.), , Distribution of Marks for Practical Examination., Time: 4 – 6 hours, Exercise- I, Exercise- II, Exercise- III, Viva-Voce, Record, , Marks: 50, ……….., 12, ……….., 12, ……….., 12, .……….., 07, .……….., 07, -----------------------Total:, 50, , Books Recommended:, 1. Introduction to Forensic Science in Crime Investigation By Dr. (Mrs.) Rukmani Krishnamurthy., 2. Computer Forensics: Principles and Practices by Linda Volonino, Reynaldo Anzaldua and Jana Godwin Pearson Prentice-Hall 2007., 3. Digital Evidence and Computer Crime, 2nd ed. By Eoghan Casey- Acdemic Press, 2004., 4. Scene of the Cybercrime: Computer Forensics Handbook by Syngress., 5. Operating system by Willam Stalling., 6. Computer Networking by Tanenbaum., 7. Computer Security Basics By Rick Lehtin., 8. Digital Forensics: Digital Evidence in Criminal Investigations by Angus McKenzie Marshall., 9. Cyber Forensic A Field Manual for Collecting, Examining and Preserving Evidence of Computer Crimes, by Albert J Menendez. Auerbach Publications., 10. Cyber Forensic by Marecella Menendez., 11. Computer Forensic by Newman., 12. Cyber Crime Investigation Field Guide, by B Middleton., 13. E-Commerce: The Cutting Edge of Business, Kamlesh K. Bajaj & Debjani Nag, Tata McGraw Hill., 14. Cyber Law and E .Commerce, David Baumer, J C Poindexter, TMG Cyberlaw Simplified Vivek Sood,, TMG., 15. E- Security, Electronic Authentication and Information Systems Security Sundeep Oberoi, TMG., 16. Firewalls and Internet Security: Repelling the Wily Hack., *****, , Appendix-C, Syllabus Prescribed for B.Sc. Final (Sem-V & VI) to be implemented from the, Academic Session 2017-18, Semester V, 5S : Animation, Advanced Graphics & Special Effects, Unit-I, , :, , Adobe After Effects: introduction to compositing, explaining tool box with all types of tools:, selection, orbit, track x-y camera, track z camera, anchor, grids, opacity, order, layer menu,, timeline, etc., , Unit-II, , :, , Use of layer menus: effects, color key, etc; nested composition, preserve resolution, preserve, frame rate, details of masking., Advanced keying and matting.

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 49, ----------------------------------------------------------------------------------------------------------------------------------------Unit-III : Animation-1: Manipulating speed, toggle hold key frame, key frame interpolation, key frame, velocity, handles, etc., Animation-2: Time stretch, remapping, linking layers and transformation., Effects: study of all types of effects., (explain each effect practically and let the student perform with it)., Unit-IV : Adobe Premiere Pro: Introduction to video production and broadcasting techniques, basics of, video composting and editing, measuring video time, detailed study of video technology, its types, like NTSC, PAL, SECAM, etc. (Only introduction of these types is expected)., Encoding and recording video signals., Unit-V : Video & real time streaming, brief idea of interlaced and non-interlace video, spatial, compression, keying, etc. Study of different windows, basic editing and concept of transition,, study of different types of video effects. (Detailed study of each with practical approach is, expected)., Unit-VI : Introduction to Sound Forge, audio concepts, working with audio engineering. Processes and, special effects via audio recording, saving the recorded file in different file formats like .mp3,, ,wav, .wma, etc., Concepts of remixing. Creating instrumental remix, title scores. Looped sound, working the, background sounds in web pages and in other applications, Practicals : Minimum eight experiments based on above contents are to be performed., Recommended Books :, 1. Recommended Text Book: Adobe After CS3 Profesional by Adobe Creative Team, Published by Adobe, Press, 2009., 2. Recommended Text Books: Digital fashion illustration with Photoshop and Illustrator by Kevin Tallon;, Published by Batsford 2008., 3. Reference books: Real word Adobe Illustrator CS4 by Mordy Golding; Published by Pretence-Hall of, India, 2008., 4. Creative Suite 3 integration: Photoshop, Illustrator by Keith Martin; Published by Pretence-Hall of India,, 2008., 5. Special edition using Adobe Photoshop 7 by Peter Bauer, Jeff Foster; Published by Pretence-Hall of India,, 2008., The Concerning teachers are also suggested to use other relevant material available on the net, to update the, knowledge of the students…, Following are the recommended links, for further search1) www.tatamcgrawhill.com, 2) www.books.google.co.in, 3) www.penguinbooksindia.com, 4) www.bookcafe.in, 5) www.newindianbooks.com, 6) www.newasiabooks.org, Semester VI, 6S : Animation, Introduction to 3D Animation, Unit-I, : Autodesk 3D Max: introduction to Autodesk 3Dmax, standard and extended primitives, cloning, managing, and hierarchy, array, floaters., Unit-II, : Concept of segments, WSM and OSM and 3D modifiers-1, 3D modifiers-2. 2D shapes, SPLINE modeling1, SPLINE modeling-2 and modifiers for shapes. Study of HSDS, FFD, poly and creating a fighter plane,, compound objects., Unit-III : Study of surfaces, patch, NURBS, all types of materials, ray tracing, architectural material and design viz., Map scalar and UVW mapping, render to texture, unwrap UVW, standard light-1, standard-2., Unit-IV : Advanced 3D Max: Photometric lights, sky light and light tracer, environment exposure control, different, effects, sun light and day light effects. Types of mental rays, RAM player and rendering techniques, using, camera and camera map modifier, pixel based camera mapping,, Unit-V, : Different types of video posts, controlling with motion panel, different types of attribute holders and wire, parameters, curve editor. Interactive animation control, animation modifier, hierarchies and kinematics, IK, and FK etc; types of schematic views, study of human anatomy, human body rigging, creating walk-cycle, and using rigging, skin and skin morphing, skin wrap and skin wrap patch., Unit-VI : Autodesk Maya : Introduction to NURBS modeling, basic dynamics used, brief idea of Maya Unlimited:, hair, fur, cloth, fluid, etc., (Brief introduction of each topic is expected only. This approach may be with or without practical)., Practicals : Minimum eight experiments based on above contents are to be performed., Recommended Books :, 1. 3Ds Max 2008 by Tickoo Sham, Published by Pearson Education, 2008., 2. Reference books: Introducing 3ds Max 2008 by Dariush Derakshshani, Randi Lorene Munn., 3. 3Ds Max 2008 In Simple Step, Published by Kogent Solutions Inc, 2008., 4. 3ds max 6 fundamentals by Ted Boardman, 2004., The Concerning teachers are also suggested to use other relevant material available on the net, to update the knowledge, of the students., Following are the recommended links, for further search1) www.tatamcgrawhill.com, 2) www.books.google.co.in, 3) www.penguinbooksindia.com, 4) www.bookcafe.in, 5), www.newindianbooks.com, 6), www.newasiabooks.org, *****

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 51, ----------------------------------------------------------------------------------------------------------------------------------------Unit-IV :, , A) Non-aqueous solvent behavior:, , 4L, , Inorganic solutes in organic solvents. Solvent system concept. The role of solvents in chemical, reactions, effect of physical and chemical properties. Inorganic reactions in the following nonaqueous solvents: Dinitrogen tetroxide, anhydrous sulphuric acid, bromine trifluride , reaction in, molten salts and Ionic liquids and Super critical CO2 as solvent., B) Metal-ligand equilibria in solution:, , 8L, , A brief introduction to complex equilibria , outline of thermodynamic stability of metal, complexes and factors affecting the such as temperature,dielectric constant and ionic strength,, nature of metal ion and ligand, statistical, electrostatics, chelate effect . Experimental methods for, the determination of stability constants by spectrophotometric methods (Job’s and Mole ratio),, Bjerrum’s pH metric method, polarographic method and Conductometric method. Relation, between thermodynamic parameters, (G,S,H) and their importance in complex, formation.Protonation and disscociation constant of ligand and their relationship. Mixed ligand, complex and application of mixed ligand complexes .General tratment of the determination of, formation constant of mixed ligand complexes., Unit-V, , :, , Symmetry and group theory:, , 12L, , Introduction to symmetry elements, symmetry operations, product of symmetry operations,, equivalence symmetry elements and equivalence atoms, point group, classifications of point, groups, Schoenflies symbols, identification of point groups of simple molecules like HCl, BeF2,, CO, H2O, NH3, CO2, BF3, C2H4, C2H6, C2H2Cl2, C6H6, PCl3, PCl5, [PtCl4]--, [PtCl2(NH3)2],, [CoCl2(NH3)4], [FeF6]3-substituted benzene molecules, pyridine, ferrocene, SF4, IF5, etc.,, necessary conditions for any set of elements to form a group, subgroups, classes in a group., Application of point group,. Group multiplication table, matrix representation of symmetry, elements. Reducible and irreducible representation, character of representation, character of, matrix, Conjugate matrix, Properties of irreducible representations, Great orthogonality theorem, (without proof) and it’s importance, construction of character table of C2v & C3v point group., Mulliken symbolism rules for irreducible representations & it’s applications with examples., , BOOK SUGGESTED1), 2), 3), 4), 5), 6), 7), 8), 9), 10), 11), 12), 13), 14), 15), 16), 17), 18), 19), 20), 21), 22), 23), 24), 25), 26), 27), 28), 29), 30), , S.F. A. Kettle, J. N. Murral & S. T. Teddler: Valency Theory, C.A. Coulson: Valency, J.E. Huheey :Inorganic Chemistry, F.A. Cotton& G. Wilkinson: Advanced Inorganic Chemistry 3rd, 5th & 6th Editions., A.F. Willims: Theoretical Approach in inorganic chemistry., A.Mannas Chanda: Atomic Structure and chemical Bonding, L.E. Orgel: An Introduction To transition metal chemistry, Ligand field theory, 2nd Edition., J.J.Logowski: Modern Inorganic Chemistry, B.Durrant and P.J.Durrant: Advanced Inorganic Chemistry, J.C.Bailar: Chemistry of co-ordination compounds., W.L.Jolly: Modern Inorganic Chemistry, R.S.Drago: Physical methods in inorganic chemistry., Waddington: Nonaqueous solvents., Sisler: Chemistry of nonaqueous solvents., A.K.Barnard: Therotical Inorganic Chemistry, Emeleus and Sharpe: Modern Aspect of Inorganic Chemistry., F.A.Cotton: Chemical Applications of Group theory., Jones: Elementary Co-ordination chemistry., B.N.Figgis: Introduction to Ligand field., S.F.A.Kettle: Co-ordination chemistry., M.C.Day and J.Selbin: Theoretical Inorganic Chemistry., J.Lewin and Wilkins: Modern Co-ordination chemistry., Gowarikar, Vishwanathan and Sheedar: Polymer science., H.H. Jattey and M. Orchin: Symmetry in chemistry., D.Schonaland: Molecular Symmetry in chemistry., L.H. Hall: Group theory and Symmetry in chemistry, H.H. Jattey and M. Orchin: Symmetry in chemistry, R.L.Dutta and A.Symal: Elements of magneto chemistry, Inorganic Chemistry 4th Edition, P.Atkins, Oxford University Press., Essential Trends in Inorganic Chemistry, D.M.P.Mingos, Oxford University Press

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 53, ----------------------------------------------------------------------------------------------------------------------------------------9. Stereochemistry of organic compounds- D. Nasipuri, New age international., 10. Stereochemistry of organic compounds- P.s.kalsi, New age international., 11. Frontier orbitals and organic chemical reactions-I. Fleming., 12. Orbital Symmetry – R.E.Lehr & A.P. Marchand., 13. Reactive intermediate in organic chemistry-N. S. Isaacs., 14. Stereochemistry of carbon compounds- E.L.Eliel., 15. Physical organic chemistry-J. Hine., 16. Name reaction in organic chemistry –Surrey., 17. Advanced organic chemistry – L.F.Fieser and M. Fieser., 18. Vol.I & II organic chemistry - I. L. Finar., 19. Modern organic chemistry- J.D. Roberts and M. C. Caserio., 20. The search for organic reaction pathways (Longmann), Peter Skyes., 21. Organic chemistry 5th Edition (McGraw Hill), Pine., 22. Organic chemistry (Willard Grant Press Botcon), John Mcmurry., 23. A Textbook of organic chemistry- R.K. Bansal., 24. New trends in green chemistry –V.K. Ahluwalia & M. kidwai, Anamaya publishers New Delhi., 25. Oranic Chemistry, J.Clayden, Oxford University Press., 26. Organic Chemistry, 4th Edition, G Marc Loudon, Oxford University Press., 27.. A guide book to Mechanism in Organic Chemistry:Petetr Sykes, 28. Organic Chemistry: F. A. Carrey( Part A & B), Paper - III, Physical Chemistry-I, 60 Hours (4-Hours/week)12 hours/Unit, Unit-I, , :, , Unit-II, , :, , Unit-III :, , Unit-IV :, , Unit – V :, , Total Marks-80, , Quantum Chemistry :, 12L., A) Schrodinger's equation in one dimensional box (Recapitulation), postulates of quantum, mechanics discussion of solution of Schrodinger's equation to particle in a three dimensional box,, Harmonic oscillator, Rigid Rotor. The variation theorem, linear variation principle, perturbation, theory (First order and non degenerate). Application of variation method and perturbation method, to Helium atom., B) Ordinary angular momentum, generalized angular momentum, eigen functions for angular, momentum, eigen value of angular momentum. Pauli exclusion principle. Russel-Saunders terms, & coupling schemes, Slatter-Condon parameters Numerical., Surface Chemistry :, 12L., A) Adsorption : Freundlich adsorption isotherm, Langmuir adsorption isotherm, Gibbs, adsorption isotherm, estimation of surface area (BET equation), surface films on liquids, and, catalytic activity at surfaces., B) Micelles : micellization, hydrophobic interaction, critical micellar concentration (CMC),, factors affecting the CMC of surfactants, counter ion binding to micelles, thermodynamics of, micellization-phase separation and mass models, solubilization, micro emulsion, reverse micelles., Numericals., Thermodynamics :, 12L, A) Classical Thermodynamics : Partial molar properties. Partial molar free energy, Chemical, Potential, Partial molar volume and Partial molar heat content and their significances., Determination of these quantities. Concept of fugacity and determination of fugacity. DebyeHuckel Theory for Activity coefficient of electrolytic solutions, Ionic strength,Determination of, Activity & Activity coefficient., B) Non equilibrium Thermodynamics : Thermodynamic criteria for non-equilibrium states,, entropy production and entropy flow for different irreversible processes (e.g. heat flow, chemical, reaction, coupled reactions and electrochemical reactions). Transformations of the generalized, fluxes and forces, phenomenological equations. Microscopic reversibility and Onsager's, reciprocity relation. Numericals., Nuclear Chemistry :, 12L., A) General characteristics of radioactive decay, decay kinetics, parent daughter decay growth, relationship, nuclear de-excitation, secular and transient equilibrium, -particle energy spectrum,, Geiger Nutta Law, theory of a band g decay process., B) Fission energy natural Ur reactor, classification of reactor, reactor power, critical size of, thermal reactor, excess reactivity and control, Breeder reactor, Reprocessing of spent fuel,, Recovery of Ur and Plutonium Nuclear wate management., Chemical Dynamics :, 12L., A) Theories of reaction rates : Collision theory, collision rates in gases, energy requirement and, steric requirement. Dynamics of molecular collisions. Transition state theory : assumptions,, Statistical Mechanics and Chemical equilibrium, derivations of Eyring equation, Application of, transition state theory to reaction between atoms and molecules (e.g. The reaction H + HBr (R), H2+Br), B) Unimolecular reactions : Lindemann-Christiansen hypothesis and Hinshelwood treatment,, Marcus's extension of the RRK treatment., C) Reactions in solution, Solvent effects on reaction rate. Factors determining reaction rate,, Numericals.

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 54, ----------------------------------------------------------------------------------------------------------------------------------------BOOK SUGGESTED1., 2., 3., 4., 5., 6., 7., 8., 9., 10., 11., 12., 13., 14., 15., 16., , Physical chemistry by P. W. Atkins and Depaula 7th Edition, Introduction to Quantum chemistry by A. K. Chandra, Tata Mc, Quantum chemistry by Ira N. Levine., Molecular quantum mechanics, Vol. I & II, P. W. Atkins, Oxford University Press, 1970., Statistical thermodynamics, by T.L.Hill, Addison Wesley, 1060, Chemical thermodynamics, by F.T. Wall, W.H.Freeman & Co. 1965, Irreversible thermodynamics, Theory and applications, by K.S.Forland, T. Forland, S.KRatje, Jonny, Witey, 1988., Chemical Kinetics,by K. J. Laidler, 3rd Edition, Harper and row, 1987., Chemical Kinetics-A study of reaction rate in solution, K.Conors, V.C.H.Publkatkm 1990., Chemical Kinetics and Dynamics, By J.I.Streinfeld, J.S. Francisco & W.I.Hase, Pritice Hall, 1989., Kinetics and Mechanism of Chemical transformation, J.Rajraman, J. Kucriacose, Mc-Million, Molecular reaction Dynamics and chemical reactivity, R.D.Levine and R.B. Benstin, Oxford University, press. 1987., Physical Chemistry by Alberty and Silby, Jolly Wiley, Essential of Quantum Chemistry by Anant Raman., Introduction to Relativistic Quantum Chemistry, K.G.Dyall, Oxford University Press., Molecular Quantum Mechanics, 4th Edition, P.W.Atkins, Oxford University Press, , PAPER-IV, Modern Methods of Separation, 60 Hours (4-Hours/week)12 hours/Unit, Unit-I, , :, , Basic concepts of Analytical Chemistry :, , Total Marks-80, 12L, , Role of Analytical Chemistry: The nature of analytical chemistry, the role of analytical chemistry, , qualitative and quantitative analytical methods, Classification of analytical methods-classical &, instrumental. Types of instrumental analysis. Selecting an analytical method. Analytical balances:, (Semi micro and Micro balances) and their use in analytical chemistry, Techniques of weighing, and errors Good Laboratory Practices (GLP) : Introduction and principles of GLP,, Purification Techniques : Introduction,purification techniques for solid organic compounds,, purification techniques for liquids, chemical method of separation and purification and criteria of, purity., Principal and Methods of sampling: Theory of sampling, pit falls and problems associated with, sampling. Techniques of sampling of gases, liquids, solids and particulates. Stoichiometric, calculations based on gravimetry and titrimetry analysis of commercial samples. Transmission, and storage of samples. Effect of sampling uncertainties samplers’ responsibility, sampling, hazards., , Unit-II, , :, , 12L, Statistical Analysis: (Emphasis should be placed on numerical problems) Collection, Treatment, and presentation of analytical data. True, standard and observed value. Defination of terms in, mean and median. Errors in chemical analysis, classification of errors, nature and origin of errors., Accuracy and precession, errors in quantitative analysis and their minimization. Standard, deviation, least squares and correlation coefficients. Confidence interval and confidence limit., Graphical method of solution, parameter and variable, comparison of manual mean curve and the, computer programmed best fitting curve.Tests for rejection of data. T-test, F-test and Q-test., Significant figures and computation rules. Regression analysis and Statistical analysis of, Chemical analysis.Numerical problems., , Unit-III :, , Separation Techniques:, , 12L, , Advanced level treatment of solvent Extraction: Introduction, Liquid-liquid extraction-continuous, and counter current extractions, synergic extraction, ion-pair or ion association extraction,, Extraction by equilibrium shifts. Solid-liquid extraction, discontinuous infusion type extraction,, application to the separation of alkali and alkaline earth metals. Numericals., Ion-Exchange Separation: Fundamental properties of ion exchangers. Theory of ion exchange,, exchange capacity, screening effect, penetration of electrolytes into ion exchange resins, sorption, of complex ions Cation and Anion exchangers, Action of ion exchange resins. Ion-exchange, equilibria and ion exchange capacity. Strongly and weakly acidic cation exchangers. Strongly and, weakly basic anion exchangers. Liquid ion exchangers, chelation ion exchangers, techniques of, ion exchange, use of non aqueous solvents in one exchange separation, application of ion, exchange separation in determination of total salt concentration, removal of interfering ions,, separation of anions and metals and application in analytical chemistry. Seperation using solvent, mixture.

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 55, -----------------------------------------------------------------------------------------------------------------------------------------, , Unit IV :, , Unit V, , :, , Gas Chromatography :, 12L, Theory and Instrumentation of GC, Sample injection- Split and splitless injection, Column types,, Solid/Liquid Stationary phases, Column switching techniques, Basic and specializeddetectors,, elemental detection, chiral separations, , Gas chromatographs and chemicalanalysis, Interfacing of, gas chromatography with mass spectrometry, Applications of GLC,Use of GC-MS ,High Speed, gas chromatography, Gas- solid chromatography and problems,, High Performance Liquid Chromatography (HPLC): Theory and instrumentation of HPLC,, Optimization of column performance, Gradient elution and related procedures, Derivatization,, Mobile phase delivery system, sample injection, separation column, detectors, Interfacing HPLC, with mass spectrometry, Structure types of column packing, adsorption chromatography,, Bonded phase chromatography, reverse phase chromatography, ion–pair chromatography, ion, exchange chromatography, size exclusion chromatography, GC-MS and LC-MS, Applications, and Problems, Chemical Safety and Handling of Chemicals:, 12L, Safe working procedure and protective environment, protective apparel, emergency, procedure, and first aid, laboratory ventilation. Safe storage and use of hazardous chemicals, procedure for, working, with substances that pose hazards, flammable or explosive hazards, procedures for, working with gases at pressures above or below atmospheric – safe storage and disposal of, waste chemicals, recovery, recycling and reuse of laboratory chemicals, disposal of chemicals in, the sanitary sewer system, incineration and transportation of hazardous chemicals., Eexplosives &Chemial weapons:, Chemical explosives: Origin of explosive properties in organic compounds, classification,, characteristics-special explosives-nitrocellulose- T.N.T, Picric acid,preparation and explosive, properties of lead azide, PETN, cyclonite (RDX), Dynamite-cordite and Gunpowder., Introduction,Classification of chemical weapons, Chemical warfare agents,physical and chemical, properties,toxicity and data, Better regulation of potential chemical weapons, , BOOK SUGGESTED1. Analytical chemistry- Problems and Solution- S. M. Khopkar, New Age International Publication., 2. Day & Underwood: Quantitative Analysis., 3. Findley: Practical Physical Chemistry:, 4. A. I. Vogel A Text book of Quantitative inorganic Chemistry, ELBS, London., 5. Strouts Galfillal: Analytical chemistry, 6. Y. Lyalikov: Physocochemical Analysis, 7. S. Wilson & P. Jones: Chemical Analysis Vol I, 8. Meites and Thomas: Advance Analytical Chemistry. (Mc Graw Hill), 9. H.H.Willard ,L.L.Merritt and J.A.Dean: Instrumental Methods of Analysis (Van Nostrand)., 10. B. L. Krayer, H. H. Willard. L. Merrit, J. A. Dean & F. A. Settle: Instrumental Methods of Analysis (CBS, Publishers, Delhi, 1986), 11. R. D. Brown Instrumental Methods of Chemical Analysis (Mc Graw Hill), 12. L. R. Shyder & C. H. Harvath: An Introduction to Separation Science (Wiley Interscience), 13. F. J. Wicher Robert: Standard Methods Chemical Analysis., 14. G.L.Davis Krupadanam, D.Vijaya Prasad, K.Varaprasad Rao, KLN Reddy, C.Sudhakar, Analytical, chemistry., 15. S.M.Khopkar Analytical chemistry of Macrocyclic and supramolecular and compounds, Narosa, publication., 16. R. D. Budhiraja Separation Chemistry, New Age., 17. Kaushik & Kaushik Perspectives in Environmental Studies, New Age, 18. R.L.Peesok and L.D.Shield: Modern Methods of Chemical Analysis., 19. Data Analysis for Chemistry, D.B.Hibbert, Oxford University Press., 20. Analytical Chemistry, S.P.J. Higson, , Oxford University Press, SEMESER I, Practical - I, Organic Chemistry, Total Hours: 90 hrs. (9 Hours per week) ( 26 Laboratory Session), , Total Marks: 100, , A- Organic Synthesis: Single Stage Preparations (25 Marks), ( 8 Laboratory Session), i) ) Benzaldehyde to cinnamic acid (Perkin Reaction), ii) p-nitrobromobenzene from bromobenzene. (Nitration), iii) Dibenzal acetone from Benzaldehyde. (Aldol Condensation), iv) Anthranilic acid to 2-iodo /2-choro benzoic acid., v) m-di-nitrobenzene to m-nitroaniline (Reduction)., vi) Diel’s Alder reaction of anthracene and maleic anhydride., vii) Synthesis of dihydropyrimidinone by Green Method (Begenneli reaction), viii) Preparation of 1,1-bis-2-napthol (Radical Coupling Reaction) by Green Synthesis, ix) Oxidation: Adipic acid by chromic acid oxidation of Cyclohexanol., x) Sandmeyer reaction: p- Chlorotoulene from p-Toluidine.

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 56, ----------------------------------------------------------------------------------------------------------------------------------------Note:, i) The preparations should be carried out using (0.02 to 0.05 mole) of the starting material., ii) The yield, melting point and TLC of the recrystallized product should be recorded., iii) The sample of the purified product and TLC plate should be submitted for inspection., Scheme of Marking:, i). Yield of the crude product, ii). MP of the recrystallized product, iii). TLC of the recrystallized product, , 10, 10, 05, , B- Qualitative Organic Analysis: (30 Marks), , ( 10 Laboratory Session), , Separation, purification and identification of binary mixtures. The two components may be solid-solid, solidliquid or liquid-liquid (nonvolatile). The water soluble solid/liquid should also be given. Student should submit, the purified samples of the separated compounds and prepare a suitable derivative of the two compounds, separated out., Note : Analysis of at least ten mixtures should be carried out., Scheme of Marking:, i), ii), , Type of the mixture, Analysis of the individual components: (10 Marks for each component), a). Detection of Elements, b). Detection of functional groups, c). Determination of MP/BP, d). Preparation of the derivative, e). Identification (Spotting), , C - Quantitative Analysis: (25 Marks), i), ii), iii), iv), v), vi), vii), viii), ix), x), , 10, 02, 02, 02, 02, 02, ( 8 Laboratory Session), , Estimation of Phenol by KBr/KBrO3, Estimation of given carbonyl compound by hydrazone formation, Determination of percentage of number of hydroxyl group in an organic compound by acetylation, method., Estimation of Aspirin. (Potentiometric/Conductometric), Estimation of Streptomycin. (Colorimetric), Estimation of vit-B12. (Colorimetric), Estimation of carbohydrates, amino acids, proteins by UV-Vis spectrophotometer, Assay of Diazepam by UV-Vis Spectrophotometer, Assay of Riboflavin by UV-Vis Spectrophotometer., Determination of Hammett constants and determine its substitution effect. i) Benzoic acid, ii) p-Nitro, Benzoic acid, iii) p-Methoxy Benzoic acid, iv) p-Methyl benzoic acid, v) p-Chloro benzoic acid. (Out of, two compounds one compound must be benzoic acid and another should be substituted benzoic acid is, given to the students), Practical-I, Organic Chemistry, , Time : 6-8 Hrs. (One day Examination), , Total Marks : 100, , (1) Exercise-1 (Organic Synthesis) 25 Marks, (2) Exercise-2 (Qualitative Analysis) 30 Marks, (3) Exercise-3 (Quantitative Analysis) 25 Marks, (4) Record 10 Marks, (5) Viva-Voce 10 Marks, --------------------------------------------------------------------Total, -100 Marks, --------------------------------------------------------------------Books Suggested:, 1. Experiments and technique in organic experiments- D. Pasto, C. Johnson and M. Miller prentice Hall., 2. Maero- scale and micro-scale organic experiments-K.L. Williaman, D. C. Heath., 3. Systematic quantitative organic analysis – H. Middleton, Edward Arnold., 4. Hand book organic chemistry – quantitative and qualitative, H. Clark, Edward Arnold., 5. Practical organic chemistry –H. Dupent, Durst and George W. Gokel., 6. Textbook of practical organic chemistry-A.I. Vogel., 7. Qualitative organic Chemial analysis-A.I. Vogel., 9. Experiment organic chemistry Vol.I &II –P.R. Singh, D. S. Gupta and K.S. Bajpai., 10. Vogel’ textbook practical organic chemistry – A.R. Tatchell, John Willey., 11. Unitised experiment in organic chemistry-Ray Q Brewalter, Calven, A. Vaudenwerf and William

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 57, ----------------------------------------------------------------------------------------------------------------------------------------Semester I, Practical - II, Physical Chemistry, Total Hours: 90 hrs. (9 Hours per week), Total Marks: 100, Use of Computer Programs 5 terms of practicals: Treatment of experimental data, X-Y plots, programs with, data preferably from physical chemistry practicals. Students will operate two packages I) MS-Word and II) MSExcel., Part-A, 1. To study the surface tension-concentration relationship for solution and determination of surface excess, concentration by using Gibbs' adsorption equation., 2. To find out the molecular surface energy and the association factor of ethyl alcohol., 3. To study the effect of concentration of an electrolyte (KC1, NaCl) on solubility of an organic acid., 4. To study the kinetics of iodine clock reaction., 5. To study the reaction between acetone & iodine in presence of acids., 6. Determination of CMC of soap by surface tension method., 7. To minimize a molecule (ibuprofen of aspirin) so as to obtain a stable conformer and calculation of, various molecular properties using quantum mechanical calculations., 8. To minimize the water molecule using DFT calculation involving B3LYP basis set., Part-B, 1. To measure refractometrically average polarisablity of some common solvents., 2. To find out the order of reaction and velocity constant of inversion of cane sugar by acid polarimetrically., 3. Polarimetric determination of the specific rotation of camphor in benzene and carbon tetrachloride., 4. Determination of strength of strong and weak acid in given mixture conductometrically., 5. To determine equivalence conductance of strong electrolytes at several concentrations and verification of, 6. Debye-Huckel Onsagar principle conductometrically., 7. To study the complex formation between ferric and salicylic acid and find the formula and stability, constant of the complex colorimetrically., 8. To determine the dissociation constant of phenolphthalein colorimetrically, 9. To determine the dissociation constant of Cu (II) and Fe (III) solution photometrically bt titrating it with, EDTA, Practical-II, Physical Chemistry, Time : 6-8 Hrs. (One day Examination), , Marks : 100, , Exercise - 1 (Instrumental), 40 Marks, Exercise - 2 (Non-Instrumental), 40 Marks, Record, 10 Marks, Viva-Voce, 10 Marks, --------------------------------------------------------------------Total, 100 Marks, --------------------------------------------------------------------Books Suggested:, 1. Findley's Practical Physical Chemistry, B.P. Levitt Longman., 2. Practical Physical Chemistry, A.M. James and F.F. Prichanrd Longman., 3. Experimental Physical Chemistry, R.C. Das and B.Behra, Tata McGrawHill., 4. Advanced Physical Chemistry Experimentals Gurtu-Gurtu Pragati Prakashan, 5. Experimental Physical Chemistry, V.D. Athanale and Parul Mathur New age International, 6. Advance Practical Physical Chemistry J.B. Yadao Goel Pubs. House., 7. Experimentals in Physical Chemistry by Dr. D.VJahagirdhar., 8. Experiments in Physical Chemistry by D.P.Shoemaker., 9. Systematic experimental Physical Chemistry by Dr. T.K. Chandhekar & S.W.Rajbhoj., Semester II, Paper V, Co-ordination Chemistry, 60hrs (4hrs/week). 12hrs/unit, , Unit-I, , :, , Total Marks 80, , A) Electronic spectra:, 12L, Introduction of electronic spectra of transition metal complexes. Derivation of term symbols for, ground and excited states of dn configurations, (L-S coupling and j-j coupling), microstates, Types, of experimental recording of the spectra, Selection rule for ligand-field and charge transfer, transitions in metal complexes, Relaxation in Selection rules, Nature of electronic spectral bands,, band widths, Band intensities & factors influencing band shapes (Jahn-Teller Effect–, Spectrochemical Series–Nephelauxetic Effect),electronic spectra of transition metal complexes of, the type[ M(H2O)n]n+ spin free and spin paired ML6 complexes of other geometries with suitable, examples. Spin forbidden transitions and effect of spin-orbit coupling. Evaluation of Dq, B’ and β, parameters (Konig method), Numericals. Orgel diagrams (d1-d9 states) and Tanabe–Sugano, diagrams of d2 and d8 configurations of an octahedral environment. Charge transfer spectra & its, mechanism, Intensity of change transfer bands.

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 58, -----------------------------------------------------------------------------------------------------------------------------------------, , Unit-II, , :, , Unit-III :, , Unit-IV :, , Unit-V, , :, , B) Magnetochemistry:, Fundamental equations in molecular magnetism, magnetic susceptibility and magnetic moment;, diamagnetic and paramagnetic behavior of transition metal complexes of different geometries,, factors affecting the magnetic properties, Temperature dependence of paramagnetism(TDP) and, temperature independent paramagnetism(TIP) of complexes, High spin-low spin crossover., Abnormal magnetic properties, orbital contributions and quenching of orbital angular momentum,, spin-orbit coupling, magnetic interactions, ferromagnetism and antiferromagnetism. Anomalous, magnetic moments and magnetic exchange coupling. Magnetic properties of polynuclear, complexes. Magnetic moment, electronic spectra and structure of tetrahalocobalt(II)complexes,, tetrahedral and octahedral Ni(II) complexes., Reaction Mechanism of Transition Metal complexes-I:, 12L, Classification of Inorganic reactions, Energy profile diagram with terminology includes transition, state or activated complex, substrate, attacking reagents electrophilic and nucleophilic. Reactivity, of metal complexes, ligand replacement reaction: classification of mechanism and energy profile, of reaction. Inert and labile complexes, interpretation of liability and inertness of transition metal, complexes on the basis of VBT and CFT. Factors affecting the lability of a complex, transition, state or activated complex, substrate, attacking reagents electrophilic and nucleophilic.Kinetics of, octahedral substitution, acid hydrolysis, factors affecting acid hydrolysis, base hydrolysis,, conjugate base mechanism, direct & indirect evidences in favour of conjugate mechanism,, anation reaction, reaction without metal ligand bond cleavage, reactions of coordinated ligands., Molecular rearrangement complexes. Geometrical, linkage and optical isomerization reactions., Ligand stereospecificity., Reaction Mechanism of Transition Metal complexes-II:, `, 12L, Substitution reaction in square planer complexes: the trans effect, trans-directing series, cis effect,, steric effect, solvent effect, effect of leaving group, effect of charge, effect of nucleophile, effect, of temperature. Trans effect theories, uses of trans-effect, mechanism of substitution reactions in, Pt(II) complexes. Electron transfer reactions. Types of electron transfer reactions, conditions of, electron transfer, and mechanism of one-electron transfer reactions, outer sphere and inner sphere, mechanisms, two electron transfer reactions-complimentary and non-complimentary reactions., Tunneling effect, cross-reaction, Marcus-Hush theory, bridged activated mechanism. Synthesis of, coordination compounds using electron transfer reactions. Photochemical reaction of Chromium, and Ruthenium complexes., Metal pi-Complexes:, 12L, Metal carbonyls: Structure and bonding, structural elucidation of metal carbonyls (by IR, and, 13, C NMR spectra), important reaction of metal carbonyls. Metal carbonyl clusters with reference, to classification, EAN rule, synthesis and structures. Application of Wilkinson’s catalyst and, Vaska’s compound., Metal nitrosyls: Nitrosylating agents for synthesis of metal nitrosyls, vibrational spectra and Xray diffraction studies of transition metal nitrosyls for bonding and structure elucidation,, important reactions of transition metal nitrosyls, structure and bonding., Fluxional Organometallic compounds : Fluxionality and dynamic equilibria in compounds such, as 2-olefin, 3-allyl and dienyl complexes., Bio-inorganic chemistry:, 12L, Bioinorganic chemistry: Overview of Bioinorganic chemistry, biological role of alkali metal, ions, ligands, ion transport across the membrane, Classification as enzymatic and non-enzymatic, metals, enzymatic redox metals such as Cu(SOD) and enzymatic non redox metals such as, Zn(Hydrolase)., 5L, Bioinorganic chemistry of Fe: Hemoglobin and myoglobin, their structures and functions, their, coordination geometry and electronic structure, trigger mechanism, Introduction of Fe-S proteins,, electron transfer proteins: Rubredoxin, 2Fe-2S Ferredoxins, 4Fe-4S and 8Fe-8S proteins, Transport protein(transferrin) and storage protein(ferritin), Oxygenation reactions, Hill constant, and Bohr Effect., 5L, Bioinorganic chemistry of Co:Vitamin-B12, its structure and biochemical function and, mechanisms of action., 2L, , Suggested Books, 1., 2., 3., 4., 5., 6., 7., 8., 9., 10., 11., 12., 13., , J.E.Huheey :Inorganic Chemistry, F.A.Cotton& G. Wilkinson: Advanced Inorganic Chemistry 3rd, 5th & 6th Editions., A.F. Willims: Theoretical Approach in inorganic chemistry., Mannas Chanda: Atomic Structure and chemical Bonding, L. E. Orgel: An Introduction To transition metal chemistry, Ligand field theory, 2nd Edition., J. J. Logowski: Modern Inorganic Chemistry, B.Durrant and P.J.Durrant: Advanced Inorganic Chemistry, J C. Bailar: Chemistry of co-ordination compounds., W. L. Jolly: Modern Inorganic ChemistryJones: Elementry Co-ordination chemistry., B. N. Figgis: Introduction to Ligand field., M.C.Day and J.Selbin: Therotical Inorganic Chemistry., J. Lewin and Wilkins: Modern Co-ordination chemistry., Purcell and Kotz: Inorganic Chemistry.

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 60, ----------------------------------------------------------------------------------------------------------------------------------------Unit-V : GREEN CHEMISTRY :, 12L, Designing a green synthesis: Choice of starting material, choice of solvents. Basic principle of, green chemistry: Prevention of waste by products, Maximum incorporation of the reactants, (starting material and reagents) into the final products. Rearrangements reaction, Addition, reaction, substitution, elimination reaction, Prevention or minimization of hazardous products., Designing of safer chemical. Synthesis involving basic principles of green chemistry, some, examples-Synthesis of styrene, Synthesis of urethane, Free radical bromination ,Synthesis of, paracetamol, Synthesis of Ibuprofen., Microwave induced green synthesis: Oxidation of Toluene, Synthesis of Chalcones, Fries, rearrangement, Diels Alder reaction, Hydrolysis of benzyl chloride. Aqueous phase reactions:, Heck reaction, Benzoin condensation, Michael Reaction Bio Catalyst in organic synthesis, Ionic, Liquids as Green Solvents., Books Suggested1., 2., 3., 4., 5., 6., 7., 8., 9., 10., 11., 12., 13., 14., 15., 16., 17., 18., 19., 20., 21., 22., 23., 24., 25., 26., 27., 28., 29., 30., 31., 32., 33., 34., , Advanced organic chemistry –Reaction mechanism and structure. Jerry March, John Wiley., Advanced organic chemistry- F.A. Carey and R.J. Sunberg, Plenum., A Guidebook to mechanism in organic chemistry-Peterskyes, Longman., Structure and mechanism in organic chemistry-C.K. Gold, Cornell University Press., Organic chemistry, R.T. Morrison Boyd. Prentice Hall, Modern organic chemistry-H.O. House, Benjamin., Principal of organic chemistry-R.O.C. Norman and J.M. Coxon, Blackie Academic and Professional., Reaction mechanism in organic chemistry-S.M. Mukharji and S.P. Singh, Macmilan., Stereochemistry of organic compounds- D. Nasipuri, New age international., Stereochemistry of organic compounds- P.s.kalsi, New age international., Frontier orbitals and organic chemical reactions-I. Fleming., Orbital Symmetry – R.E.Lehr & A.P. Marchand., Reactive intermediate in organic chemistry-N. S. Isaacs., Stereochemistry of carbon compounds- E.L.Eliel., Physical organic chemistry-J. Hine., Name reaction in organic chemistry –Surrey., Advanced organic chemistry – L.F.Fieser and M. Fieser., Vol.I & II organic chemistry - I. L. Finar., Modern organic chemistry- J.D. Roberts and M. C. Caserio., The search for organic reaction pathways (Longmann), Peter Skyes., Organic chemistry 5th Edition (McGraw Hill), Pine., Organic chemistry (Willard Grant Press Botcon), John Mcmurry., A Textbook of organic chemistry- R.K. Bansal., New trends in green chemistry –V.K. Ahluwalia & M. kidwai, Anamaya publishers New Delhi., Fundamentals of photochemistry-KK Rohatgi & Mukharji, Photochemistry-Cundau & Gilbert, Aspects of organic phoptochemistry-WM horspoot, Photochemistry-JD calvert, Photochemistry-RP Wayne R. M. Acheson : An introduction to chemistry of heterocyclic compounds, (Interscience)., Pericyclic Reactions and organic photochemistry, Green Solvents for organic synthesis: V. Ahluwalia& R. S. Verma, Eco Friendly Synthesis of fin Chemicals: Roberto Ballini, Essentials of molecular photochemistry, A. Gilbert and J. Baggott. Blackwell Scientific Publication., Molecular photochemistry, N.J. Urro, W. A. Benjamin, Paper - VII, Physical Chemistry - II, , 60hrs (4hrs/week). 12hrs/unit, , Total Marks 80, , Unit-I, , :, , Chemical Dynamics :, A) Kinetics of Complex reactions: Chain reaction (H2+Br, ® 2 HBr thermal and photo chemical, reaction), Homogeneous catalysis (acid-base and enzymes), oscillating reactions (BelousovZhabotinsky reaction, Lotka-Volterra mechanism, the brusselator and the oregonator)., 6L, B) Fast reactions: General features of fast reactions, Stopped flow method, relaxation method,, Nuclear magnetic resonance method, Flash Photolysis, Numericals., 6L, , Unit-II, , :, , Quantum Chemistry :, A) Construction of M.O.by LCAO for H2+ ion, Calculation of energy levels from wave, functions, physical picture of bonding & anti-bonding wave functions, concept of orbitals and, their characteristics., 6L, B) Hybride orbitals sp, sp2, sp3;Calculationof coefficient of A.O. used in hybride orbital;Huckel, theory of Conjugated systems, bond order & charge density calculations. Applications to, ethylene, butadiene, cyclopropenyl radical, cyclo- butadiene. Numericals., 6L

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 61, ----------------------------------------------------------------------------------------------------------------------------------------Unit-III : Macromolecules:, A) Definition of macromolecule (Polymer), types of polymers, Random coils, configuration and, conformation of macromolecules, electrically conducting molecular wires, fire resistant, liquid, crystal polymers, kinetics of polymerization, mechanism of polymerization. stability of biological, polymers, Application of polymers., 6L, B) Number average & mass average molecular mass, molecular mass determination by, Osmometery, Viscometry, Ultracentrifugation, light scattering & size-exclusion chromatography, method, Numericals, 6L, Unit-IV : Electrochemistry :, A) Electrochemistry of solutions: Debye-Huckel-Onsager treatment and its extension. Ion solvent, interactions.. Bio-electrochemistry, Introduction, threshold membrane phenomenon, Nernst Plank Equation, Hodges Huxley equation, core conductor models, electrocardiography., 6L, B) The rate of charge transfer, the Butler-Volmer equation, the low overpotential limit the high, overpotential limit, Tafel plot. Voltammetry, Concentration polarization,, experimental, techniques, corrosion, Types of corrosion, corrosion inhibitors , Corrosion monitoring. and, prevention methods. Numericals., 6L, Unit-V : Statistical Thermodynamics :, A) Thermodynamic probability, most probabale distribution. Maxwell-Boltzmann distribution, law Fermi-Dirac statistics, distribution law and applications to metals. Bose-Einstein statistics distribution law and application to helium., 6L, B) Partition function- Translational, rotational, vibrational and electronic partition functions,, calculations of thermodynamic properties in terms of partition functions. Applications of partition, functions. Numericals., 6L, List of Books:, 1. Physical chemistry by P.W.Atkins & dePaula 7th Edition, 2. Molecular reaction Dynamics and chemical reactivity, R.D.Levine, and R.B. Benstin, Oxford University Press. 1987., 3. Physical Chemistry by Alberty and Silby, Jolly Wiley, 4. Adsorption and Catalysis by solids, by D.K.Chakraburti, Wiley Eastern, 1990, 5. The Theory of Adsorption and catalysis, by A. Clark, Academic press, 1970, 6. Micells Theoretical and applied aspects, by V.Moroy. Plenum, 7. Modern Electrochemistry by A.K.N.Raddy, 8. Theoretical electrochemistry by D.LAntropov, Mir Publisher WJ2, 9. Electrochemistry by J. Dvorak, J. Koryta, V. Bohackova., 10. Introduction to radiation chemistry by J.W.T. Spinks and RJ.Woods, Paper VIII, Optical Methods and Environmental Chemistry, 60hrs(4hrs/week), 12hrs/Unit, Unit-I, , :, , 80Marks, , Optical Method, 12L, Spectrophotometry and Colorimetry: Brief introduction of topic,Application of, spectrophotometric metods for study of composition of coloured complex ,Multiple analysis, Pk, value of indicator etc. Photometric titrations. Applications of quantitative and qualitative analysis,, problems., Principles, Plane polarized and circularly polarized rays, optical rotation, optically active molecules, optical rotator d, Theory, instrumentation and applications of fluorimetry, Nephelometry, turbidimetry, Polarimetry, & Refractometry., Unit II : Flame Emission and atomic spectrometry:, 12L, Flame photometry: Elementary theory of flame photometry. Instrumentation and experimental, techniques. Interferences, analytical techniques and applications. Atomic absorption spectrometry, (AAS): introduction, principles, Advantages of AAS over FES, Instrumentation, Flame, atomization. Hallow cathod lamps, interferences and applications. Comparison of atomic, absorption with atomic emission methods., UNIT-III : WATER POLLUTION :, 12L, Origin of wastewater, types, water pollutants and their effects. Sources of water pollution,, domestic, industrial, agricultural soil and radioactive wastes as sources of pollution. Objective of, analysis, parameter for analysis colour, turbidity, total solid, conductivity, acidity, alkalinity,, hardness, chloride, sulphate, fluoride, silica, phosphates and different forms of nitrogen. Heavy, metal pollution, public health significance of Cadmium, Chromium, Copper, zinc Lead,, Manganese, Mercury and Arsenic.General survey of instrumental technique for the analysis of, heavy metals in aqueous systems. Oxygen content of water and aquatic life. Measurments of DO,, BOD, COD and their significance as pollution indicators. Pesticides as water pollutants and, analysis. A brief idea of coagulation and flocculation., Unit IV : AIR POLLUTION, 12L, Sources and sinks of gases pollutants, classification of air pollutants, effect of air pollutants on, living and non-living things. Sources of air pollution, air quality standards and sampling. Analysis, of air pollutants (CO, CO2, NOx, SOx, H2S ,NH3 and Hydrocarbons and particulates). Green, house effect, acid rain, ozone depletion and their consequences on environment. Effects of air, pollution, photochemical smog and monitoring of air pollution.

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 62, ----------------------------------------------------------------------------------------------------------------------------------------Unit-V :, , Soil Pollution and Pesticide Analysis, 12L, Chemistry of soil, soil irrigation by effluents. Agricultural pollution, role of micronutrients in soil, trace, element analysis in soil, Pesticides and pollution. Sources of pesticide residue in the environment, classification of pesticides,, pesticide degradation by natural forces, effect of pesticide residue on life. Analytical techniques for pesticide, residue analysis. DDT problem., Radiation pollution-Classification and effects of radiation. Effects of ionizing radiation on Man. Effect of, nonionizing radiation on life. Radioactivity and nuclear fall out, protection and control from radiation., , List of Books, 1. Analytical chemistry- Problems and Solution- S. M. Khopkar, New Age International Publication., 2. Day & Underwood: Quantitative Analysis., 3. Findley: Practical Physical Chemistry:, 4. Vogel A Text book of Quantitative inorganic Chemistry, ELBS, London., 5. Strouts Galfillal: Analytical Y. Lyalikov: Physocochemical Analysis, 6. S. M.Khopkar:Basic concep in Analytical Chemistry, 7. Meites and Thomas: Advance Analytical Chemistry. (Mc Graw Hill), 8. H.H.Willard ,L.L.Merritt and J.A.Dean: Instrumental Methods of Analysis (Van Nostrand)., 9. B. L. Krayer, H. H. Willard. L. Merrit, J. A. Dean & F. A. Settle: Instrumental Methods of Analysis, (CBS Publishers, Delhi, 1986), 10. R. D. Brown Instrumental Methods of Chemical Analysis ,McGraw Hill, 11. L. R. Shyder & C. H. Harvath: An Introduction to Separation Science (Wiley Interscience)., 12. Environmental chemistry, S. E. Manahan, Lewis Publishers., 13. Environmental chemistry, Sharma & Kaur, Krishna publishers., 14. Environmental chemistry, A. K. De, Wiley Eastern., 15. Environmental Pollution Analysis, S. M. Khopkar, Wiley Eastern., 16. Environmental Toxicology, Ed. J. Rose, Gordon and Breach Science Publication., 17. Elemental Analysis of Airborne Particles, Ed. S. Landberger and M. Creatchman, Gordon and breach, Science Publication., 18. Atmospheric pollution, W. Buch, McGraw Hill, New York., 19. Fundamentals of Air Pollution, S. J. Williason, Addison – Wesley Publishers., 20. Analytical Aspect of Environmental chemistry, D. F. S. Natush and P. K. Hopke. John Wiley & sons., New York., 21. Analytical chemistry- Problems and Solution- S. M. Khopkar, New Age., 22. Environmental Chemistry, J.W.Vanloon, Oxford University Press., 23. E. Stocchi: Industrial Chemistry, Vol-I, Ellis Horwood Ltd. UK., 24. R.M. Felder, R.W. Rousseau: Elementary Principles of Chemical Processes, Wiley Publishers, New Delhi., 25. J. A. Kent: Riegel’s Handbook of Industrial Chemistry, CBS Publishers, New Delhi., 26. S. S. Dara: A Textbook of Engineering Chemistry, S. Chand & Company Ltd. New Delhi., 27. K. De, Environmental Chemistry: New Age International Pvt., Ltd, New Delhi., 28. S. M. Khopkar, Environmental Pollution Analysis: Wiley Eastern Ltd, New Delhi., 29. S.E. Manahan, Environmental Chemistry, CRC Press (2005).  G.T. Miller, Environmental Science 11th, edition. Brooks/ Cole (2006)., 30. A. Mishra, Environmental Studies. Selective and Scientific Books, New Delhi (2005)., Semester II, Practical - III, Physical Chemistry, Total Hours: 90 hrs. (9 Hours per week), Total Marks: 100, Use of Computer Programs 5 terms of practicals:, Treatment of experimental data, X-Y plots, programs with data preferably from physical chemistry practicals. Students will, operate two packages I) MS-Word and II) MS-Excel., Part-A, 1., Determination of radius of molecules of glycerol by viscometry., 2., Determine the viscosity of unknown mixture of two liquids by viscometry (ethyl alcohol + water), 3., Study the influence of ionic strength on the solubility of CaSO4 and hence to determine thermodynamic solubility, product and mean ionic activity., 4., Determine rate constant of reaction between potassium persulphate and potassium iodide having equal concentration, of reacting species., 5., Investigate the autocatalysis reaction between KMnO4 and oxalic acid and calculate the energy of activation., 6., Investigate the solubility of three component system and hence draw a tie line on binodal curve., 7., Study the variation of solubility of Ca(OH)2 in pressure of NaOH solution. Hence determine solubility product at, room temperature., 8., Determination at surface excess of amyl alcohol by capillary rise method., 9., Part-B, 10. Determine Hammett constant of a given substituted benzoic acid by pH measurement., 11. To determine the hydrolysis constant of active hydrochloride by pH measurement., 12. To determine pH of butter solution using quinhydrone electrode., 13. Determination of pK value of aid-base indicator (methyl red, methelene blue and bormo cresol) by, spectrophotometrically., 14. Determination of standard electrode potential of Zinc and Copper., 15. To find the strength of HCl and Acetic acid in given mixture potentiometrically., 16. To find the strength of mixture of halides by titrating it against AgNO3 solution potentiometrically., 17. To determine the hydrolysis constant of aniline chloride by emf method.

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----------------------------------------------------------------------------------------------------------------------------------------, , SANT GADGE BABA AMRAVATI UNIVERSITY GAZETTE - 2017 - PART TWO - 63, -----------------------------------------------------------------------------------------------------------------------------------------, , Practical-III, Physical Chemistry, Time : 6-8 Hrs. (One day Examination), Marks : 100, Exercise - 1 (Based on Part-A), 40 Marks, Exercise - 2 (Based on Part-B), 40 Marks, Record, 10 Marks, Viva-Voce, 10 Marks, --------------------------------------------------------------------Total, 100 Marks, --------------------------------------------------------------------Physical Chemistry Practical, Books Suggested:, 1) Experimental physical chemistry, R.C. Das and B. Behera, Tata McGraw-Hill, 2) Advanced physical chemistry J.B. yadao, Goel Pub House, 3) Experiments in physical Chemistry D.P. Shormaker, C.W. Garland and J.W. mbler, Tata McGraw Hill, Comp., 4) Post graduate physical chemistry, Patel, Turakhia, Kelkar, Himalaya Pub House, 5) Experiments, in physical chemistry, D.V. Jahagirdar, Himalaya Pub House, 6) Practical Physical Chemistry, A. Findlay Revised by J.A. Kitehner, Longmans, Green, 7) Experiments in Physical Chemistry, F. Daniels and J. Williams, Mc Graw Hill., 8) Systematic Experimental Physical Chemistry, T.K. Chondekar & S.W. Rajbhoj, Anjali Pub. Aurangabad., 9) Advanced Physical Chemistry Experiments,, J.N. Gurtu & A. Gurtu, Pragati Prakashan, 10) Practical Physical Chemistry, A.M. James & P.E. Prichard, Longam Group Ltd., 11) Experiments in physical Chemistry, J.M.Wilson, KJ.Newcombe, A.R. Denko, and R.M.W.Richett,, Pergamon Press,, 12) Senior Practical Physical Chemistry, B.D.Khosle and V.S. Garg S.Chand & Comp., Semester II, Practical IV, Inorganic Chemistry Practicals, Practical Work load 9 Hrs. /Week, , Marks 100, , I], , Preparation of inorganic compounds by greener methods and their characterization by elemental, analysis, MW determination, decomposition temperatures and molar conductance studies., (Minimum 9), 1. [VO (acac) 2], 2. Preparation of bis(acetylacetonato)copper(II)., 3. Preparation of tris (acetylacetonato) iron (III)., 4. Preparation of tris (acetylacetonato) manganese (III)., 5. Cis K [Cr (C2O4) 2(H2O) 2], 6. Na [Cr (NH3) 2(SCN) 4], 7. K3 [Fe (C2O4) 3], 8. Hg [Co (SCN) 4], 9. [Co (Py) 2 Cl2], 10. [Ni (DMG) 2], 11. TiO (C9H8NO) 2(H2O) 2, 12. Cis [Co (trine)(NO2) 2] Cl H2O, 13. [Cu2 (CH3COO) 4(H2O) 2], 14. K3 [Al (C2O4) 3](H2O) 3, 15. Preparation and characterization of Isomers of Tris (8-Hydroxyquinolinato) aluminium (III) complex, II] A) Quantitative Analysis of mixture of two cations:, Quantitative analysis of binary mixture of cations involving their chemical separation and separate analysis, of one cation by gravimetry and another by volumetric or colorimetric. Certain model examples are given, below:, i), Copper (II) and Nickel (II), ii), Copper (II) and Zinc (II), iii), Nickel (II)—Zinc (II), iv), Copper (II)—Iron (III), B) Analysis of Limestone, Dolomite and Bauxite., III] Qualitative analysis of radicals, Qualitative analysis of inorganic mixture for a total of five radicals including interfering radicals (not more, than one such radical in a mixture), rare earth (not more than two rare earths in a mixture) and combination, of cations (minimum 8 mixtures)., Cations: Mercury (I, II), Pb, Ag, Bi (III), Cu (II), Cd (II), As (IV, V), Sb (IV, V), Sn (II, IV), Fe (III), Al, (III), Cr (III), Ni (II), Co (II), Mn (II), Zn (II), Barium, Strontium, Calcium and Magnesium., Interfering radicals: Phosphate, Oxalate, Fluoride and Borate., Rare Earth: Tl, Mo, W, Se, Ti, Zr, Th, V, U, Ce.